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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 526479Generated: October 30, 2026

Ethylamine → HCID 178464867, compound

https://huagongshe.com/reaction/526479

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthylamineHCID 6341—
ReactantHCID 178426451HCID 178426451—
ProductHCID 178464867HCID 178464867—

Reaction Steps

The title compound was prepared in a manner similar to Example 74 using 6-(4-(4-cyano-2-methylphenyl)-5-hydroxy-1H-pyrazol-1-yl)nicotinic acid and ethanamine. 1H NMR (400 MHz, DMSO-d6) δ ppm 1.09 (t, J=7.33 Hz, 3H) 2.36 (s, 3H) 3.16-3.37 (m, 2H) 7.59 (d, J=8.08 Hz, 1H) 7.66 (s, 1H) 7.71 (br. s., 1H) 7.99-8.22 (m, 1H) 8.34 (d, J=7.58 Hz, 2 H) 8.65 (t, J=5.05 Hz, 1H) 8.78-8.90 (m, 1H) 12.84-13.41 (m, 1H). MS m/z [M+H]+348.1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09345713B2
Source datasetuspto-grants-2016_05
ORD IDord-7556463406844db3a06bbd7a5ad988fe
Source noteuspto-grants-2016_05