HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-benzyl-6-hydrazinylpyridine-3-carboxamide → HCID 178509610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-benzyl-6-hydrazinylpyridine-3-carboxamide | HCID 51370238 | — |
| Reactant | Ethyl 2-(2-chloro-4-cyanophenyl)-3-(dimethylamino)acrylate | HCID 117601384 | — |
| Product | HCID 178509610 | HCID 178509610 | — |
Reaction Steps
The title compound was prepared in a manner similar to Example 188 using ethyl 2-(2-chloro-4-cyanophenyl)-3-(dimethylamino)acrylate and N-benzyl-6-hydrazinylnicotinamide. 1H NMR (400 MHz, DMSO-d6) δ ppm 4.44 (d, J=5.8 Hz, 2H) 7.13-7.22 (m, 2H) 7.27 (d, J=4.3 Hz, 5H) 7.75 (d, J=8.3 Hz, 1H) 8.00 (s, 1H) 8.30-8.47 (m, 2H) 8.90 (s, 1H) 9.20 (t, J=5.3 Hz, 1H). MS m/z [M+H]+ 430.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09345713B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-19fc1727cbdf4b39a203449c4e85a506 |
| Source note | uspto-grants-2016_05 |