HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-[2-(2-Methoxyethoxy)ethoxy]acetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (2-(2-Methoxyethoxy)ethoxy)acetic acid | HCID 85241 | — |
| Product | 2-[2-(2-Methoxyethoxy)ethoxy]acetyl chloride | HCID 2759571 | — |
Reaction Steps
Thionyl chloride, 8.0 grams (0.112 mole) was stirred, and 10.0 grams (0.056 mole) of 3,6,9-trioxadecanoic acid was added dropwise during a 45 minute period. Upon completion of addition, the reaction mixture was warmed to reflux where it stirred for 45 minutes. The reaction mixture was cooled, yielding 3,6,9-trioxadecanoyl chloride. An 80% yield of acid chloride was assumed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05616718 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-73a3327c0951477183f87214e9224beb |
| Source note | uspto-grants-1997_04 |