HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 71477447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | HCID 86717345 | HCID 86717345 | — |
| Product | HCID 71477447 | HCID 71477447 | 96% |
Reaction Steps
A solution of 2-amino-2-(4-isopropyl-2-methoxyphenyl)-2H-inden-1,3-dione (0.80 g, 2.58 mmol) in anhydrous THF (20 ml) was added triphosgene (0.84 g, 2.84 mmol) and stirred for 15 min. The reaction mixture was concentrated and was dissolved in ethanol (20 ml) was stirred for 2 hrs at room temperature to afford the title compound (0.95 g, 96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346749B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-f6fb36ac244a412a9ad9ed900b756f26 |
| Source note | uspto-grants-2016_05 |