HCID 86711622, compound → HCID 86711632, compound

HRID 527361Notes

Reaction equation

HRID 527361 reaction equation
FC1C=C(C=CC=1S(C)(=NC#N)=O)CN1C(=[O:15])C2C(=CC=CC=2)C1=O.[C:26]([O:30][C:31](=[O:46])[NH:32][CH2:33][C:34]1[CH:39]=[CH:38][C:37]([S:40]([CH3:44])=[N:41][C:42]#[N:43])=[CH:36][C:35]=1[F:45])([CH3:29])([CH3:28])[CH3:27]>>[C:26]([O:30][C:31](=[O:46])[NH:32][CH2:33][C:34]1[CH:39]=[CH:38][C:37]([S:40]([CH3:44])(=[N:41][C:42]#[N:43])=[O:15])=[CH:36][C:35]=1[F:45])([CH3:29])([CH3:27])[CH3:28]

Participants

3

Reactant 2

HCID 86711622HCID 86711622, compoundHCID 86711631HCID 86711631, compound

Product 1

HCID 86711632HCID 86711632, compound

Procedure

The title compound is prepared following the procedure described for preparation 15c, using (2-fluoro-4-(N-cyano-S-methylsulfinimidoyl)-benzyl)-carbamic acid tert-butyl ester (preparation 18c) as starting material. ESI mass spectrum: [M+H]+=312; r.t. HPLC: 0.68 min (5-95AB).

Workup

  1. customr.t

Sources & evidence

ORD record
ord-0c02ab4635a7496db0fa811e7f4d7eae
Source dataset
uspto-grants-2016_05
Patent number
US09346794B1

Reaction notes

Loading…