HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-(N-Cyanomethyl-S-methylsulfonimidoyl)benzyl)isoindoline-1,3-dione → 4-(N-cyanomethyl-S-methylsulfonimidoyl)benzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-(N-Cyanomethyl-S-methylsulfonimidoyl)benzyl)isoindoline-1,3-dione | HCID 86711638 | — |
| Reactant | 4-(Aminomethyl)-N,N,N'-trimethylbenzenesulfonimidamide | HCID 89978813 | — |
| Product | 4-(N-cyanomethyl-S-methylsulfonimidoyl)benzylamine | HCID 89978755 | — |
Reaction Steps
The title compounds is prepared in analogy to preparation 60d, using 2-(4-(N-cyano-methyl-S-methylsulfonimidoyl)benzyl)isoindoline-1,3-dione (preparation 64a) as starting material. ESI mass spectrum: [M+H]+=224; r.t. HPLC: 0.22 min (X011_S03).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346794B1 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-2e25dfcbea6c4041a14f522f6dc4aa06 |
| Source note | uspto-grants-2016_05 |