HuagongsheHuagongshe Chemistry Print Report · For research reference only
Di(succinimido) carbonate → HCID 131730601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Di(succinimido) carbonate | HCID 676246 | — |
| Reactant | 1,1-Dimethylethyl N-[2-[[[(4-aminophenyl)amino]carbonyl]amino]ethyl]carbamate | HCID 67121275 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 131730601 | HCID 131730601 | 114.3% |
Reaction Steps
N,N′-Disuccinimidylcarbonate (5.49 g, 21.44 mmol, 1.1 eq) was added at room temperature to a stirred solution of N-(4-aminophenyl)({2-[(tert-butoxy)carbonylamino]ethyl}amino)carboxamide (6.75 g, 19.49 mmol, 1.0 eq) in CH3CN (350 mL). After stirring overnight at room temperature, the reaction mixture was filtered and to afford 9.70 g of the expected crude product as a light brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346799B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-0e47d127a2824683bc183ea7d2c56aaa |
| Source note | uspto-grants-2016_05 |