Chloroacetic Acid → HCID 86750633, compound

HRID 52763Notes

Reaction equation

HRID 52763 reaction equation
S([CH2:5][C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH3:34])=[O:7])(O)(=O)=O.[Na].[Cl:36]CC(O)=O>>[Cl:36][CH2:5][C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH3:34])=[O:7]

Participants

3

Reactant 2

HCID 300Chloroacetic AcidHCID 86750634Sodium lauryl-myristyl sulfoacetate

Product 1

HCID 86750633HCID 86750633, compound

Conditions

Temperature
93 °C

Procedure

The reactor is then heated to a temperature of 93° C. and maintained at a temperature of between 90° C. and 97° C. for about 11 hours. HPLC analysis of the resulting slurry indicates that the sodium lauryl-myristyl sulfoacetate is substantially free of monochloroacetic acid and its salts.

Workup

  1. temperaturemaintained at a temperature of between 90° C. and 97° C. for about 11 hours

Sources & evidence

ORD record
ord-fc07395c622945258f6551f71b391f76
Source dataset
uspto-grants-1997_04
Patent number
US05616782

Reaction notes

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