HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Isothiocyanate → HCID 86667796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Isothiocyanate | HCID 2346 | — |
| Reactant | HCID 57477268 | HCID 57477268 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86667796 | HCID 86667796 | — |
Reaction Steps
4-(3,8-Diaza-bicyclo[3.2.1]oct-3-yl)-7H-pyrrolo[2,3-d]pyrimidine (intermediate 4) (0.05 mmol) was dissolved in THF (1 mL), and benzyl isothiocyanate (0.06 mmol) was added. The reaction mixture was left at rt for 16 hours. The pure compounds were obtained by standard preparative HPLC purification of the reaction mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346809B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-e64cc6563f5544dbb1ceab750334d3a8 |
| Source note | uspto-grants-2016_05 |