HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 86718878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 86718879 | HCID 86718879 | — |
| Product | HCID 86718878 | HCID 86718878 | 100.1% |
Reaction Steps
Following a procedure analogous to that for the synthesis of Intermediate 31B, 5-(tert-butoxycarbonylamino)naphthalene-2-sulfonic acid (Intermediate 31A, 3.70 g, 11.44 mmol) and N-chlorosuccinimide (1.60 g, 12.01 mmol) were converted to the title compound (2.95 g, 90%). MS(ESI+) m/z 275.1 (M+NH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346795B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-27330be751fd4b908fb1086cdfbbad1f |
| Source note | uspto-grants-2016_05 |