HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 71062377, compound → HCID 71060740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 71062377 | HCID 71062377 | — |
| Reactant | HCID 86718952 | HCID 86718952 | — |
| Product | HCID 71060740 | HCID 71060740 | 70% |
Reaction Steps
Following a procedure analogous to that for the synthesis of Intermediate 291B, 3-tert-butyl 1-methyl 4-(2-chloropyrimidin-4-yl)isophthalate (244 mg, 0.70 mmol) was converted to the title compound (210 mg, 70% for two steps). MS(ESI+) m/z 428.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346795B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-79770d2eced94734a5e322f4c2649737 |
| Source note | uspto-grants-2016_05 |