HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl Formate → HCID 68763133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl Formate | HCID 61207 | — |
| Reactant | Butyl 5-(2-ethoxy-2-oxoethyl)spiro[indole-3,4'-piperidine]-1'-carboxylate | HCID 69810198 | — |
| Product | HCID 68763133 | HCID 68763133 | — |
Reaction Steps
tert-butyl 5-(2-ethoxy-2-oxoethyl)spiro[indoline-3,4′-piperidine]-1′-carboxylate was prepared by the procedures described in Example 1, Step 2, substituting tert-butyl 5-chlorospiro[indole-3,4′-piperidine]-1′-carboxylate with butyl 5-(2-ethoxy-2-oxoethyl)spiro[indole-3,4′-piperidine]-1′-carboxylate. LCMS (APCI+) m/z 275.2 [M+H−Boc]+; Rt=3.58 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346805B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-0f16b993c01745e283264e850836d300 |
| Source note | uspto-grants-2016_05 |