HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68760523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 68761380 | HCID 68761380 | — |
| Product | HCID 68760523 | HCID 68760523 | 72% |
Reaction Steps
A solution of (1′-benzyl-1-(4-methoxybenzyl)spiro[indoline-3,3′-pyrrolidine]-4-yl)methanamine (0.500 g, 1.21 mmol) in TFA (7.00 mL) was heated at 85° C. for 24 hours. The solvent was evaporated to give (1′-benzylspiro[indoline-3,3′-pyrrolidine]-4-yl)methanamine trifluoroacetic acid salt (0.355 g, 0.872 mmol, 72%). LCMS (APCI+) M+H+ 294 (100%); Rt=2.06 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346805B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-8a53f97628fd456b94cb6a2d95f1f656 |
| Source note | uspto-grants-2016_05 |