HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone → 1-Hydroxycyclohexyl phenyl ketone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | epsilon-CAPROLACTONE | HCID 10401 | — |
| Reactant | Acrylate | HCID 25188 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | 1-Hydroxycyclohexyl phenyl ketone | HCID 70355 | — |
Reaction Steps
To 900 parts by weight of methyl ethyl ketone were added 100 parts by weight of cyclohexanone, 750 parts by weight of partially caprolactone-modified polyfunctional acrylate (DPCA-20, produced by Nippon Kayaku Co., Ltd.), 200 parts by weight of a silica sol (MIBK-ST, produced by Nissan Chemical Industries, Ltd.) and 50 parts by weight of a photopolymerization initiator (IRGACURE 184, produced by Ciba Specialty Chemicals Corp.), followed by stirring. The mixture was filtered through a polypropylene filter having a pore size of 0.4 μm to prepare Coating solution A for hardcoat layer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346961B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-2d8e5089e0994b5fb3d83d603eccece6 |
| Source note | uspto-grants-2016_05 |