HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → (S,Z)-3-Amino-1-benzyl-3,4-dihydro-1H-azepin-2(7H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | (S,Z)-3-amino-1-benzyl-3,4,7,8-tetrahydroazocin-2(1H)-one | HCID 68292242 | — |
| Product | (S,Z)-3-Amino-1-benzyl-3,4-dihydro-1H-azepin-2(7H)-one | HCID 68292696 | — |
Reaction Steps
(S,Z)-3-Amino-1-benzyl-3,4-dihydro-1H-azepin-2(7H)-one (6.15 mg, 0.028 mmol) was synthesized as described for the preparation of Intermediate 44 using prop-2-en-1-amine in step A. Anal. Calcd. for C13H16N2O m/z 216.2. found: 217.0 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346852B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-9d27a4fc0eaa4534824af22e107eed24 |
| Source note | uspto-grants-2016_05 |