HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Allyl-ortho-toluidine → (S,Z)-3-Amino-1-o-tolyl-3,4-dihydro-1H-azepin-2(7H)-one trifluoroacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Allyl-ortho-toluidine | HCID 250708 | — |
| Reactant | (S,Z)-3-Amino-1-phenyl-3,4-dihydro-1H-azepin-2(7H)-one trifluoroacetate | HCID 68292369 | — |
| Product | (S,Z)-3-Amino-1-o-tolyl-3,4-dihydro-1H-azepin-2(7H)-one trifluoroacetate | HCID 86706225 | — |
Reaction Steps
(S,Z)-3-Amino-1-o-tolyl-3,4-dihydro-1H-azepin-2(7H)-one trifluoroacetate (17 mg, 0.051 mmol) was synthesized as described for the preparation of Intermediate 52 using N-allyl-2-methylaniline in step A. Anal. Calcd. for C13H16N2O m/z 216.2. found: 217.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346852B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-bb79addc1be94b9cbe67f48b064c64fa |
| Source note | uspto-grants-2016_05 |