Triethylamine → HCID 57914362, compound

Participants

Reaction Steps

As in the synthesis of N-(2-azidoethyl)tetradecanamide, (0.338 g, 1.23 mmol) was reacted with 2-azidoethanamine (0.106 g, 1.23 mmol) and triethylamine (0.249 g, 2.46 mmol) in dichloromethane (5 mL) to give N-(2-azidoethyl)palmitamide (0.336 g, 84% yield). 1H NMR (300 MHz, CDCl3) δ 6.11 (s, 1H), δ 3.41 (s, 4H), δ 2.17 (t, J=7.5 Hz, 2H), δ 1.60 (m, 2H), δ 1.23 (m, 2H), δ 0.85 (t, 6.3 Hz, 3H) ppm; 13C NMR (75 MHz, CDCl3) δ 173.9, 51.1, 39.1, 36.9, 32.1, 29.9, 29.8, 29.8, 29.7, 29.6, 29.5, 25.9, 22.9, 14.3 ppm; HRMS (ESI) calcd for C18H36N4O (M+) 324.2889. found 324.2879.

Provenance & Evidence