HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19036213, compound → HCID 178494670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19036213 | HCID 19036213 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178494670 | HCID 178494670 | 52.5% |
Reaction Steps
Following a procedure similar to that described in Example 82(b), but detritylating 2.5 g of (5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 4-(1-hydroxy-1-methylethyl)-2-methoxymethyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate [prepared as described in step (a) above] with a 25% v/v aqueous solution of acetic acid, 916 mg of the title compound were obtained as crystals, melting at 138°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05616599 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-478c3356ae4b46a2b574075a1da9d308 |
| Source note | uspto-grants-1997_04 |