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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 52993Generated: October 30, 2026

HCID 19036213, compound → HCID 178494670, compound

https://huagongshe.com/reaction/52993

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19036213HCID 19036213—
SolventAcetic AcidHCID 176—
ProductHCID 178494670HCID 17849467052.5%

Reaction Steps

Following a procedure similar to that described in Example 82(b), but detritylating 2.5 g of (5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 4-(1-hydroxy-1-methylethyl)-2-methoxymethyl-1-{4-[2-(trityltetrazol-5-yl)phenyl]phenyl}methylimidazole-5-carboxylate [prepared as described in step (a) above] with a 25% v/v aqueous solution of acetic acid, 916 mg of the title compound were obtained as crystals, melting at 138°-140° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05616599
Source datasetuspto-grants-1997_04
ORD IDord-478c3356ae4b46a2b574075a1da9d308
Source noteuspto-grants-1997_04