Chlorosuccinimide → 2-(5-(3-Chloropyrazolo[1,5-a]pyridin-2-yl)pyridin-3-yl)propan-2-ol

Participants

Reaction Steps

A solution of the title compound from Example 2 Step A (0.099 g, 0.391 mmol) and N-chlorosuccinimide (0.063 g, 0.469 mmol) in acetonitrile (1.95 ml) was stirred at room temperature for 2 hours. The reaction was then concentrated under reduced pressure, diluted with dichloromethane, washed with saturated aqueous sodium chloride solution, dried over MgSO4, filtered and concentrated under reduced pressure.

Provenance & Evidence