HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 530135Generated: October 25, 2026
Chloro(diphenyl)silane → Benzyl 5-(chlorodiphenylsilyl)pentanoate
https://huagongshe.com/reaction/530135
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chloro(diphenyl)silane | HCID 74206 | — |
| Reactant | 4-Pentenoic acid, phenylmethyl ester | HCID 10052035 | — |
| Product | Benzyl 5-(chlorodiphenylsilyl)pentanoate | HCID 90418864 | — |
Reaction Steps
To a mixture of chlorodiphenylsilane (0.49 g; 2.58 mmol) and benzyl pent-4-enoate (0.50 g; 2.58 mmol) under argon was added two drops of Karstedt's catalyst solution (in xylenes; ˜2% Pt). The reaction vessel was sealed and the mixture was heated to 60° C. for 15 hours. The crude liquid was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09352049B2 |
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| Source dataset | uspto-grants-2016_05 |
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| ORD ID | ord-6cd526816cce4681ae3f154cca16a097 |
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| Source note | uspto-grants-2016_05 |
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