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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 530137Generated: October 25, 2026

4-Pentenoic acid, phenylmethyl ester → HCID 90417926, compound

https://huagongshe.com/reaction/530137

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Pentenoic acid, phenylmethyl esterHCID 10052035—
Reactant1-ChlorosilolaneHCID 71364168—
ProductHCID 90417926HCID 90417926—

Reaction Conditions

Temperature60 °C

Reaction Steps

To a mixture of crude 1-chlorosilolane (0.317 g) and benzyl pent-4-enoate (0.50 g; 2.63 mmol) under argon was added two drops of Karstedt's catalyst solution (in xylenes; ˜2% Pt). The reaction vessel was sealed and the mixture was heated to 60° C. for 18 hours. The crude liquid was used without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09352049B2
Source datasetuspto-grants-2016_05
ORD IDord-822de5eb39cf41d8a61145a148ccab26
Source noteuspto-grants-2016_05