Potassium Hydroxide → HCID 117720216, compound

HRID 530236Notes

Reaction equation

HRID 530236 reaction equation
[CH3:1][C:2]1([C:10]([O:12]CC)=[O:11])[CH2:6][CH2:5][C:4]([CH3:8])([CH3:7])[C:3]1=[O:9].[OH-].[K+:16]>CO>[CH3:1][C:2]1([C:10]([O-:12])=[O:11])[CH2:6][CH2:5][C:4]([CH3:7])([CH3:8])[C:3]1=[O:9].[K+:16]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 89600959HCID 89600959, compound

Product 1

HCID 117720216HCID 117720216, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To a stirred solution of the product of Example 8b (6.72 g, 33.9 mmol) in methanol (34 mL) was added a cooled aqueous potassium hydroxide solution (1.0 M, 68 mL, 68 mmol). The reaction was then stirred at room temperature overnight. The material was used directly for the next step.

Sources & evidence

ORD record
ord-eaeeeaf43c444ec8886885dd00f7b2b5
Source dataset
uspto-grants-2016_05
Patent number
US09353063B2

Reaction notes

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