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HRID53028

反应详情

EQUATION

反应方程式

HRID 53028 的结构方程式

REACTANTS

反应物

3
结构：CCOCC
HCID3283

Diethyl Ether

C4H10O

结构：CCCc1nc(C#N)c(C#N)n1C(c1ccccc1)(c1ccccc1)c1ccccc1
HCID19036122

2-Propyl-1-(triphenylmethyl)-1H-imidazole-4,5-dicarbonitrile

C27H22N4

结构：CC[Mg]Br
HCID178418443

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1nc(C(=O)CC)c(C#N)n1C(c1ccccc1)(c1ccccc1)c1ccccc1
HCID19036223

未命名化合物

PROCEDURE

实验过程

Following a procedure similar to that described in Preparation 15, but using 8.05 g of 2-propyl-1-tritylimidazole-4,5-dicarbonitrile (prepared as described in Preparation 14) and 14 ml of a 3M solution of ethylmagnesium bromide in diethyl ether, 7.03 g of the title compound were obtained as crystals, melting at 96° C. (softening at 87° C.).

WORKUP

后处理

  1. customthat described in Preparation 15