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HRID53039

反应详情

EQUATION

反应方程式

HRID 53039 的结构方程式

REACTANTS

反应物

2
结构：O=C1OC(Br)c2ccccc21
HCID96218

1(3H)-Isobenzofuranone, 3-bromo-

C8H5BrO2

结构：CCCc1nc(C(C)(C)O)c(C(=O)O)[nH]1
HCID178440085

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1nc(C(C)(C)O)c(C(=O)OC2OC(=O)c3ccccc32)[nH]1
HCID178440074

未命名化合物

收率 94.8%

PROCEDURE

实验过程

Following a procedure similar to that described in Preparation 31, but using 1.06 g of 4-(1-hydroxy-1-methylethyl)-2-propylimidazole-5-carboxylic acid [prepared as described in Preparation 22(i)] and 1.15 g of 3-bromophthalide, 1.63 g of the title compound were obtained as an amorphous solid.

WORKUP

后处理

  1. customthat described in Preparation 31