Potassium Carbonate → HCID 117600334, compound

Participants

Reaction Conditions

Reaction Steps

1-Bromo-3-(phenylethynyl)benzene (3 g, 11.7 mmol), 3-pyridylboronic acid (1.6 g, 13.0 mmol), Tetrakis(triphenylphosphine)palladium (0.3 g, 0.26 mmol) and potassium carbonate (3.2 g, 23.2 mmol) were dissolved in N,N-dimethylformamide and the reaction was stirred at 100° C. overnight under nitrogen. The mixture was extracted with dichloromethane and the combined organic phases were washed with water, dried over sodium sulfate and concentrated in vacuo to give the title compound as oil (1.3 g, 43% yield).

Provenance & Evidence