Butanedioic acid, lithium salt (1:2) → Lithium Lysine Succinate

HRID 53071Notes

Reaction equation

HRID 53071 reaction equation
O.[NH2:2][C@H:3]([C:9]([OH:11])=[O:10])[CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].[C:12]([O-:19])(=[O:18])[CH2:13][CH2:14][C:15]([O-:17])=[O:16].[Li+:20].[Li+]>O>[C:12]([O-:19])(=[O:18])[CH2:13][CH2:14][C:15]([O-:17])=[O:16].[NH2:2][C@H:3]([C:9]([OH:11])=[O:10])[CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].[Li+:20].[Li+:20]

Participants

4

Reactant 2

HCID 10197702Butanedioic acid, lithium salt (1:2)HCID 16211825Lysine Monohydrate

Product 1

HCID 86750663Lithium Lysine Succinate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

10 grams of L-lysine monohydrate are dissolved in 25 ml of water, 8.1 grams of lithium succinate is added and dissolved. The solution is then dried in a 110° C. oven until solids begin to form when cooled to room temperature. After 15 to 30 minutes solids form at room temperature and are collected.

Workup

  1. dissolutiondissolved
  2. customThe solution is then dried in a 110° C. oven until solids
  3. customto form when
  4. customAfter 15 to 30 minutes solids form at room temperature
  5. customare collected

Sources & evidence

ORD record
ord-619ebf0aaedf4d899675749b204b857e
Source dataset
uspto-grants-1997_04
Patent number
US05618467

Reaction notes

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