L-Lysine monohydrochloride → Lysine Magnesium Succinate

HRID 53074Notes

Reaction equation

HRID 53074 reaction equation
O.[NH2:2][C@H:3]([C:9]([OH:11])=[O:10])[CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].Cl.N[C@H](C(O)=O)CCCCN.[C:23]([O-:30])(=[O:29])[CH2:24][CH2:25][C:26]([O-:28])=[O:27].[Mg+2:31]>O>[C:23]([O-:30])(=[O:29])[CH2:24][CH2:25][C:26]([O-:28])=[O:27].[Mg+2:31].[NH2:2][C@H:3]([C:9]([OH:11])=[O:10])[CH2:4][CH2:5][CH2:6][CH2:7][NH2:8]

Participants

5

Reactant 3

HCID 69568L-Lysine monohydrochlorideHCID 10219480Magnesium succinateHCID 16211825Lysine Monohydrate

Product 1

HCID 86750665Lysine Magnesium Succinate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
-20 °C

Procedure

Dissolve 10.0 grams of lysine monohydrate in 10 ml of hot water (60° C.). Add 11.1 grams of lysine monohydrochloride and 17.1 grams of magnesium succinate and bring to a boil for 5 minutes. This viscous gel is then frozen in a freezer at -20° C. for 5 minutes. The frozen solid gives a bright blue green phosphorescence when excited under a long wave UV light with a lifetime of 15-20 seconds similar to the dried solid.

Workup

  1. customThe frozen solid gives a bright blue green phosphorescence when
  2. customexcited under a long wave UV light with a lifetime of 15-20 seconds similar to the dried solid

Sources & evidence

ORD record
ord-9e62b11591f04ec79b7bb7b57c4cbce3
Source dataset
uspto-grants-1997_04
Patent number
US05618467

Reaction notes

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