Thionyl Chloride → 3-(Chloromethyl)-2,6-dimethylpyridine

Beteiligte Stoffe

Reaktionsschritte

The solution of compound (2,6-dimethylpyridin-3-yl)methanol (0.76 g, 5.6 mmol) in SOCl2 (5 mL) was stirred at room temperature for 1 hour and then concentrated to give the crude product 3 which was used for next step directly without further purification. LCMS (ESI) m/z=156.1 (M+H)+.

Herkunft & Nachweise