Sodium Bicarbonate → HCID 118662859, compound

Participants

Reaction Steps

A solution of compound 2 (180 mg, 0.39 mmol) in TFA (5 mL) was stirred at room temperature for 2 h, then pH was adjusted to 7-8 with saturated NaHCO3 solution. Extracted with EtOAc (20 mL*3) and washed with H2O and brine, the organic phase was concentrated to give the title compound. ESI-MS: 341.2 (M+H)+.

Provenance & Evidence