HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → Tert-butyl 3-(benzylimino)cyclohexylcarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | (3-Oxo-cyclohexyl)-carbamic acid tert-butyl ester | HCID 44228975 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Tert-butyl 3-(benzylimino)cyclohexylcarbamate | HCID 67983484 | — |
Reaction Steps
A reaction mixture of tert-butyl 3-oxocyclohexylcarbamate (4 mmol, 852 mg) and benzylamine (4 mmol, 436 μL) in refluxing toluene (25 mL) in a Dean-Stark apparatus was stirred for overnight. The product, tert-butyl 3-(benzylimino)cyclohexylcarbamate, was obtained after evaporation of solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09351965B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-c67beb7f762c4bcfb3d68e185e07aaae |
| Source note | uspto-grants-2016_05 |