HCID 68106186, compound → HCID 15800439, compound

Participants

Reaction Steps

To a solution of 3 (3.67 g, 7.64 mmol) in ethanol (60 mL) was added 10% Pd/C (1.10 g). The resulting mixture was stirred under H2 (g) atmosphere at room temperature for 12 hours. The reaction mixture was filtered through a celite pad and washed with ethanol (2×10 mL). The combined filtrate was evaporated in vacuo to give an oily residue which was triturated with Et2O to provide an off-white solid 4 (1.57 g, 97% yield).

Provenance & Evidence