HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15379646, compound → 3-CYANOMETHYL-6-ACETYLOXAZOLO[4,5-b]PYRIDIN-2(3H)-ONE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15379646 | HCID 15379646 | — |
| Reactant | 6-Bromo-3-methyl[1,3]oxazolo[4,5-b]pyridin-2(3H)-one | HCID 15926016 | — |
| Product | 3-CYANOMETHYL-6-ACETYLOXAZOLO[4,5-b]PYRIDIN-2(3H)-ONE | HCID 19079295 | — |
Reaction Steps
The method of operation is the same as that used for the synthesis of the compound of Example 1 (coupling with 1-ethoxy-1-(trimethylstannyl)ethylene). 6-bromo-3-(cyanomethyl)oxazolo[4,5-b]pyridin-2(3H)-one from Preparation 3 is used instead of the 6-bromo-3-methyloxazolo[4,5-b]pyridin-2(3H)-one from Preparation 2. The yield obtained is 60%. ##STR48##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05618819 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-4a2456cfabda4a5e92719b985a4a7763 |
| Source note | uspto-grants-1997_04 |