N-BOC-ethylenediamine → HCID 58413406, compound

HRID 532313Notes

Reaction equation

HRID 532313 reaction equation
[CH3:1][O:2][C:3]([C:5]1[S:27][C:8]2[N:9]=[CH:10][N:11]=[C:12]([NH:13][C:14]3[CH:19]=[CH:18][C:17]([F:20])=[CH:16][C:15]=3[O:21][CH:22]([C:24]([OH:26])=O)[CH3:23])[C:7]=2[C:6]=1[CH3:28])=[O:4].[NH2:29][CH2:30][CH2:31][NH:32][C:33](=[O:39])[O:34][C:35]([CH3:38])([CH3:37])[CH3:36]>>[CH3:1][O:2][C:3]([C:5]1[S:27][C:8]2[N:9]=[CH:10][N:11]=[C:12]([NH:13][C:14]3[CH:19]=[CH:18][C:17]([F:20])=[CH:16][C:15]=3[O:21][CH:22]([C:24](=[O:26])[NH:29][CH2:30][CH2:31][NH:32][C:33]([O:34][C:35]([CH3:38])([CH3:37])[CH3:36])=[O:39])[CH3:23])[C:7]=2[C:6]=1[CH3:28])=[O:4]

Participants

3

Reactant 2

HCID 187201N-BOC-ethylenediamineHCID 58413270HCID 58413270, compound

Product 1

HCID 58413406HCID 58413406, compound

Procedure

Prepared analogously to example 56.1 using the product from 55 (170 mg) and tert-butyl N-(2-aminoethyl)carbamate (90 μl).

Sources & evidence

ORD record
ord-f46e471a48934190bb62c9d2d9471412
Source dataset
uspto-grants-2014_10
Patent number
US08853193B2

Reaction notes

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