Benzamide → HCID 21192648, compound

HRID 532379Notes

Reaction equation

HRID 532379 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12])[C:5]([OH:7])=O.[C:15](N)(=O)C1C=CC=CC=1>>[Cl:1][C:2]1[CH:3]=[C:4]([C:5](=[O:7])[CH3:15])[CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12]

Participants

3

Reactant 2

HCID 2331BenzamideHCID 2400533-Chloro-4,5-dimethoxybenzoic acid

Product 1

HCID 21192648HCID 21192648, compound

Procedure

3-Chloro-4,5-dimethoxybenzoic acid (1 g) was converted to the benzamide derivative analogously to O3.043, and the latter to the title compound analogously to O2.059. 495 mg of the title compound were obtained. LC-MS rt: 1.55 min [M+H]+: 215.1 (met. a)

Sources & evidence

ORD record
ord-514645e736e94448a038afcb55938c14
Source dataset
uspto-grants-2014_10
Patent number
US08853206B2

Reaction notes

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