8-Methyl-8-azabicyclo(3.2.1)octan-3-ol → HCID 68944112, compound

HRID 532429Notes

Reaction equation

HRID 532429 reaction equation
[CH3:1][N:2]1[CH:7]2[CH2:8][CH2:9][CH:3]1[CH2:4][CH:5]([OH:10])[CH2:6]2.F[C:12]1[CH:17]=[CH:16][C:15]([N+:18]([O-:20])=[O:19])=[CH:14][C:13]=1[CH3:21]>>[CH3:1][N:2]1[CH:7]2[CH2:8][CH2:9][CH:3]1[CH2:4][CH:5]([O:10][C:12]1[CH:17]=[CH:16][C:15]([N+:18]([O-:20])=[O:19])=[CH:14][C:13]=1[CH3:21])[CH2:6]2

Participants

3

Reactant 2

HCID 84248-Methyl-8-azabicyclo(3.2.1)octan-3-olHCID 68001Benzene, 1-fluoro-2-methyl-4-nitro-

Product 1

HCID 68944112HCID 68944112, compound

Procedure

8-Methyl-8-aza-bicyclo[3.2.1]octan-3-ol was reacted with 1-Fluoro-2-methyl-4-nitrobenzene according to method D. The product with the molecular weight of 276.34 (C15H20N2O3) was obtained in this way; MS (ESI) 277 (M+H+).

Workup

  1. customThe product with the molecular weight of 276.34 (C15H20N2O3) was obtained in this way

Sources & evidence

ORD record
ord-7fab5793d4954a5281f96971aed48c48
Source dataset
uspto-grants-2014_10
Patent number
US08853208B2

Reaction notes

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