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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 532810Generated: October 30, 2026

1-Bromo-2,4-dimethoxybenzene → HCID 59366192, compound

https://huagongshe.com/reaction/532810

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Bromo-2,4-dimethoxybenzeneHCID 87266—
ReactantTert-butyl 1,4-diazepane-1-carboxylateHCID 2756058—
ReactantPotassium tert-butoxideHCID 23665647—
Solvent1,2-DimethoxyethaneHCID 8071—
ProductHCID 59366192HCID 5936619244.8%

Reaction Conditions

Temperature60 °C

Reaction Steps

A mixture of 1-bromo-2,4-dimethoxybenzene (433 mg, 1.99 mmol, 1 equiv), [1,4]diazepane-1-carboxylic acid tert-butyl ester (400 mg, 1.99 mmol, 1 equiv), t-BuOK (313.7 mg, 2.79 mmol, 1.4 equiv) and allylchloro[1,3-(2,6-di-isopropylphenyl)imidazol-2-ylidene]palladium (II) (Nolan's catalyst, 11.4 mg, 0.02 mmol, 0.01 equiv) in 4 mL of DME was degassed with compressed nitrogen gas for 5 min. The resulting mixture was stirred at 60° C. overnight and cooled down to room temperature. EtOAc (˜30 mL) was added and the mixture was filtered through celite. The filtrate was washed with saturated aqueous NaHCO3 (20 mL) and brine (20 mL) sequentially and then dried over magnesium sulfate. The residue was purified by flash column chromatograph using 30 to 100% EtOAc in hexane to afford the title compound as yellowish liquid (300 mg) after evaporation and dried in vacuo. MS (ES) m/z 337.2 (M+H+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08853202B2
Source datasetuspto-grants-2014_10
ORD IDord-32d03039eed845d58224d8b20654c274
Source noteuspto-grants-2014_10