HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethylphenylisocyanate → HCID 58329478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethylphenylisocyanate | HCID 137096 | — |
| Reactant | 4-Cyclopentylamino-8-methoxy-quinoline-3-carboxylic acid ethyl ester | HCID 67249718 | — |
| Product | HCID 58329478 | HCID 58329478 | 16.5% |
Reaction Steps
1-Cyclopentyl-3-(2,3-dimethyl-phenyl)-7-methoxy-1H-pyrimido[5,4-c]quinoline-2,4-dione (22 mg) was prepared from 4-cyclopentylamino-8-methoxy-quinoline-3-carboxylic acid ethyl ester (0.32 mmol) and 1-isocyanato-2,3-dimethyl-benzene (0.48 mmol) following general procedure C. LCMS: m/z 416 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853226B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-a881ca0b25254f18bd4ad972ca96af4d |
| Source note | uspto-grants-2014_10 |