HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 67316267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Naphthalenethiol | HCID 68259 | — |
| Reactant | Ethyl 3-(3-(methylsulfonyloxy)propyl)-1h-indole-2-carboxylate | HCID 87353567 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 67316267 | HCID 67316267 | — |
Reaction Steps
A mixture of EXAMPLE 10A (42 mg), naphthalene thiol (45 mg), and potassium carbonate (36 mg) in acetonitrile (2 mL) was heated at 80° C. for 3 days. The reaction mixture was poured into water, extracted with dichloromethane and purified by flash chromatography on silica gel with 0-20% ethyl acetate in hexanes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853209B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-e1dfa09626a14fc0925b8340aa0a84fc |
| Source note | uspto-grants-2014_10 |