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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 533264Generated: October 29, 2026

Cesium carbonate → HCID 67316412, compound

https://huagongshe.com/reaction/533264

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCesium carbonateHCID 10796—
Reactant1-(3-Bromopropoxy)naphthaleneHCID 12959381—
ReactantHCID 67315809HCID 67315809—
SolventDimethylformamideHCID 6228—
SolventEthyl AcetateHCID 8857—
ProductHCID 67316412HCID 67316412—

Reaction Steps

To a solution of EXAMPLE 126B (1.14 g) and 1-(3-bromopropoxy)naphthalene (0.922 g) in N,N-dimethylformamide (20 ml) was added cesium carbonate (2.158 g). The reaction was stirred at room temperature overnight and diluted with ethyl acetate and washed with water. The organic layer was dried over sodium sulfate, filtered and concentrated. The residue was purified by flash chromatography, eluting with 0-50% dichloromethane in hexane to provide the title product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08853209B2
Source datasetuspto-grants-2014_10
ORD IDord-1d8dbaf4f1894ae19e3f7d367020eeff
Source noteuspto-grants-2014_10