HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium formate → Diethyl 5-(4-fluorophenoxy)-1,3-benzenedipropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium formate | HCID 2723923 | — |
| Reactant | HCID 53975825 | HCID 53975825 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Diethyl 5-(4-fluorophenoxy)-1,3-benzenedipropanoate | HCID 19962382 | 70.6% |
Reaction Steps
Treatment of diethyl 3,3'-[5-(4-fluorophenoxy)-1,3-phenylene]bis-2-propenoate (17.0 g) with ammonium formate (27.85 g) and 10% of palladium on carbon (1.70 g) according to the method of Preparation 12 gave the title compound as an oil (12.12 g), Rf 0.30 (SS 1). Found: C,68.01; H,6.46. C22H25FO5 requires C,68.03; H,6.49%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05618941 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-db053f4549434b5fa820e85cee0cd16b |
| Source note | uspto-grants-1997_04 |