HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178497322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 178497323 | HCID 178497323 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178497322 | HCID 178497322 | 88% |
Reaction Steps
A mixture of methyl 4-hydroxyquinoline-6-carboxylate (2.07 g), N-chlorosuccinimide (1.36 g), and acetic acid (56 mL) was stirred at room temperature for one day. The reaction mixture was diluted with water, and then, the precipitate was collected by filtration to obtain methyl 3-chloro-4-hydroxyquinoline-6-carboxylate (2.13 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853242B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-6b1b42788d7b4d80a849a9ab49c16cbe |
| Source note | uspto-grants-2014_10 |