HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl formate → n-(2,3-Dihydro-benzo[1,4]dioxin-2-ylmethyl)-formamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl formate | HCID 8025 | — |
| Edukt | 2-Aminomethyl-1,4-benzodioxane | HCID 15053 | — |
| Produkt | n-(2,3-Dihydro-benzo[1,4]dioxin-2-ylmethyl)-formamide | HCID 64990658 | — |
Reaktionsschritte
Racemic 2,3-dihydro-1,4-benzdioxin-2-ylmethylamine (825 mg, 5 mmol) was dissolved in ethyl formate (15 mL), refluxed for 30 min and evaporated in vacuo to yield N-(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-formamide as an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08853263B2 |
| Quelldatensatz | uspto-grants-2014_10 |
| ORD ID | ord-6cc8b543205e4bba9d3f104a6dceb232 |
| Quellennotiz | uspto-grants-2014_10 |