Potassium Carbonate → HCID 46843216, compound

Participants

Reaction Steps

3-Chloro-6,7,8,9-tetrahydro-5H-dipyrido[2,3-b;3′,4′-d]pyrrole (50 mg; 0.24 mmol), 3-(bromomethyl)benzonitrile (56 mg; 0.29 mmol), and K2CO3 (0.04 ml; 0.72 mmol) where dissolved in DMF (2 ml) and stirred overnight at room temperature. Prep-LC-MS purification provided 16 as an off-white powder (21 mg, 27% yield). LC-MS (M+H=323, obsd.=323).

Provenance & Evidence