HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 46843217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Methoxybenzyl bromide | HCID 4067207 | — |
| Reactant | HCID 66677239 | HCID 66677239 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 46843217 | HCID 46843217 | 18% |
Reaction Steps
3-Chloro-6,7,8,9-tetrahydro-5H-dipyrido[2,3-b;3′,4′-d]pyrrole (50 mg; 0.24 mmol), 3-methoxybenzyl bromide (0.04 ml; 0.29 mmol), and K2CO3 (0.04 ml; 0.72 mmol) were dissolved in DMF (2 ml) and stirred overnight at room temperature. Prep-LC-MS purification provided 17 as an off-white powder (14 mg, 18% yield). LC-MS (M+H=328, obsd.=328).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853391B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-ae959ca61a044973b4004ddd9dfe5ab2 |
| Source note | uspto-grants-2014_10 |