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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 533734Generated: October 30, 2026

Potassium Carbonate → HCID 46843217, compound

https://huagongshe.com/reaction/533734

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant3-Methoxybenzyl bromideHCID 4067207—
ReactantHCID 66677239HCID 66677239—
SolventDimethylformamideHCID 6228—
ProductHCID 46843217HCID 4684321718%

Reaction Steps

3-Chloro-6,7,8,9-tetrahydro-5H-dipyrido[2,3-b;3′,4′-d]pyrrole (50 mg; 0.24 mmol), 3-methoxybenzyl bromide (0.04 ml; 0.29 mmol), and K2CO3 (0.04 ml; 0.72 mmol) were dissolved in DMF (2 ml) and stirred overnight at room temperature. Prep-LC-MS purification provided 17 as an off-white powder (14 mg, 18% yield). LC-MS (M+H=328, obsd.=328).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08853391B2
Source datasetuspto-grants-2014_10
ORD IDord-ae959ca61a044973b4004ddd9dfe5ab2
Source noteuspto-grants-2014_10