Water → HCID 46843444, compound

Participants

Reaction Steps

4-Methoxybenzenesulfonyl chloride (0.04 mL, 0.26 mmol) was added to a solution of 3-chloro-6,7,8,9-tetrahydro-5H-dipyrido[2,3-b;3′,4′-d]pyrrole (50 mg, 0.24 mmol) in pyridine (2 mL), and the reaction was stirred overnight at room temperature. The reaction mixture was added to water (20 mL), and the resulting precipitate was filtered and dried under vacuum to provide 39 (61 mg, 67% yield) as a yellow solid. LC-MS (M+H=379, obsd.=379).

Provenance & Evidence