HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Bromobutoxy)benzene → HCID 11692149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Bromobutoxy)benzene | HCID 70986 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11692149 | HCID 11692149 | 64.9% |
Reaction Steps
Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0604 g, 0.206 mmol) and 4-bromobutyl phenyl ether (0.106 g, 0.463 mmol) in 2 CH3CN/3 CHCl3 (5.0 mL) were reacted to give the desired product (0.0649 g, 64.9%). EI-MS m/z 442(M+) Rt (2.13 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853404B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-2f10e03c9c2d467ba5d5953453a80b47 |
| Source note | uspto-grants-2014_10 |