HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dibromopropane → HCID 11591329, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dibromopropane | HCID 8001 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11591329 | HCID 11591329 | 43.1% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0979 g, 0.334 mmol) and 1,3-dibromopropane (0.35 mL, 3.448 mmol) in 2 CH3CN/3 CHCl3 (15.0 mL) were reacted to give the desired product (0.0712 g, 43.1%). EI-MS m/z 415(M+) Rt (1.79 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853404B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-006a98835f9849909d1737f98de392dc |
| Source note | uspto-grants-2014_10 |