HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-1-hexene → HCID 11626675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-1-hexene | HCID 75906 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11626675 | HCID 11626675 | 67.1% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0637 g, 0.217 mmol) and 6-bromo-1-hexene (0.050 mL, 0.373 mmol) in 2 CH3CN/3 CHCl3 (5.0 mL) were reacted to give the desired product (0.0664 g, 67.1%). EI-MS m/z 376(M+) Rt (1.90 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853404B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-a90b691bca964f76b7432be4168b9be0 |
| Source note | uspto-grants-2014_10 |