HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, ((2-bromoethoxy)methyl)- → HCID 11699451, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, ((2-bromoethoxy)methyl)- | HCID 73833 | — |
| Reactant | HCID 68959827 | HCID 68959827 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11699451 | HCID 11699451 | 53.2% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl[bis(4-methylphenyl)]methanol (0.0525 g, 0.163 mmol) and 2-bromoethyl phenylmethyl ether (0.0387 mL, 0.245 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0465 g, 53.1%). EI-MS m/z 456(M+) Rt (2.09 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853404B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-e2853ad4411c4ee09bce1e93ba520fe7 |
| Source note | uspto-grants-2014_10 |