Monobenzone → HCID 86715098, compound

HRID 533907Notes

Reaction equation

HRID 533907 reaction equation
[OH:1][C@H:2]1[CH2:6][CH2:5][NH:4][C:3]1=[O:7].[CH2:8]([O:15][C:16]1[CH:21]=[CH:20][C:19](O)=[CH:18][CH:17]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>>[CH2:8]([O:15][C:16]1[CH:21]=[CH:20][C:19]([O:1][C@@H:2]2[CH2:6][CH2:5][NH:4][C:3]2=[O:7])=[CH:18][CH:17]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 7638MonobenzoneHCID 11029774(3S)-3-hydroxypyrrolidin-2-one

Product 1

HCID 86715098HCID 86715098, compound

Procedure

Typical Procedure 3 was followed. Reaction of (S)-3-hydroxy-pyrrolidin-2-one with 4-benzyloxy-phenol provided the subtitle compound. MS ESI+: m/z=284 [M+H]+.

Sources & evidence

ORD record
ord-c749f4f171b6492fad1b67a814afe231
Source dataset
uspto-grants-2014_10
Patent number
US08853412B2

Reaction notes

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